Actually, I want to synthesis FeOF from FeF3.3H2O precursor with hydrothermal methode just mix FeF3.3H2O and 1 propanol and autoclave 200 C 24h but the result always contain with some impurity FeF2, do you know how to remove that FeF2? as we know at autoclave we don't know the pressure or temp. on there because if pressure up temp will be increase too so how we can control our condition on that autoclave?