I need this for a review: What is the most popular or established method for preparation of samples for electron microscopy if a sample is hazardous for humans, e.g. when forming aerosols or is potentially infectious?
Probably not useful in your case, but a FIB is often used to prepare samples of radioactive materials for TEM. The activity of the resulting sample can be reduced by several orders of magnitude. A good paper describing the technique is "Implementation of FIB system in characterization of nuclear fuels and materials," by Aitkaliyeva, Miller and Cole (2014).