How to remove residual solvents from the CBD crystals?

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I synthesized Graphene oxide Two times but I got Peak at 8 degree first time. And second time I got a Peak at 6 degree. What will be possible reasons?

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HAs anyone used TGA to find activation enegy of water evaporation?

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Solvent recovery after extraction - Separation of Isopropanol + Water - how to do it best?

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Rob Darrington

Use a vacuum desiccator, such as:

https://www.belart.com/suggested-search/product/desiccators.html

Ensure that as you dry you has as high a surface area as possible. A skin or crust can lock in solvent.

Kind regards.

Rob

S Kalaiselvan

Dear Muzamal Iqbal

Vacuum pressure and heat are applied to a thin film of oil, allowing it to evaporate before condensing and accumulating in a receiver flask or other capture vessel.