I used fullprof software fo the refinement of xrd data. Is there any way to know the density from the software.
You can find the density of every single refined phase at the beginning of the generated ".SUM" file
I am working on a grignard reagent(PhMgBr) addition reaction(with alpha,beta unsaturated ketone) and my product is a tertiary alcohol. I have found through Tlc, I had got a mixture.How to purify...
21 April 2024 8,582 0 View
can any one explain me the procedure for the preparation of tertiary alcohols by the addition of ketone to the Grignard reagent, so that i can get the pure product. Also please suggest me the best...
21 April 2024 5,207 0 View
What is the maximum yield of colanic acid has been produced? and What is the best method of producing Colanic acid? Tell me the process, production, purification, characterization, and removal...
23 March 2024 9,032 0 View
Like in Lung cancer how b cells are getting affecting, so just want to how and what are the complications B cells are facing regarding different type of cancerous cells
06 December 2023 6,132 1 View
I there any data on the monthly rainfall in the Southern Western Ghats during 2011 and 2012?
06 August 2023 6,295 0 View
I read one or two articles about systematic reviews conducted in descriptive/ epidemiological studies, but those articles were published in 2000 and 2010 respectively. So I want to be sure about...
11 September 2022 4,290 2 View
In xrd I got crystalline peak at 28.65. Whether this peak corresponds to graphite?
11 March 2022 8,633 4 View
I have been doing work on seedling stomata. the old images cannot be measured in um but can in pixel. so I need to convert the measurement to um.
30 September 2020 8,201 4 View
Mycorrhiza is a obligate symbionts so it can not grow without root. I found it in many research article.
04 September 2020 5,242 5 View
here I wanted to study each dimension of marketing efforts that online retailers use to reduce customers perceived risk categories as follows; Financial marketing efforts like COD, payment...
25 July 2020 8,697 5 View
One of the papers I read by Toby, where (title of the paper was "R factors in Rietveld analysis: How good is good enough?"), he tells us that to get good chi square value, you must have low Rwp,...
17 July 2024 9,668 4 View
I am new to Fullprof and trying to perform a Rietvied analysis of a rare-earth zirconate sample. I was informed that one of the parameters to evaluate whether the results are acceptable is by...
10 July 2024 5,827 1 View
Hi, my research involves in ZnO synthesis. I have performed rietveld refinement of my samples and obtain a good fit using Fullprof suite software. However to obtain the crystallite size, the IRF...
07 July 2024 3,526 3 View
I am trying to refine my data in full prof and my chi2 is 0,834E11 and everytime i try to refine the data the plot deviates further from the actual data and the chi2 doesnt change. The first image...
02 June 2024 5,805 5 View
I have synthesized strontium based hydroxy-apatite by co-precipitation process. i have done the rietveld refinement of it. The problem is its chi-square is not less than 2, even though I have...
10 May 2024 2,566 5 View
fullprof
26 March 2024 6,499 0 View
I have a concern regarding readjusting the intensities value of xrd data. In one the discussion in this platform, (the link is here-...
11 March 2024 7,680 1 View
Using TOF method of neutron diffraction data to process crystal phase, I have converted gsas prm file into irf, and added manual background, the data is doped, why is the Prague Summit missing...
26 February 2024 8,413 1 View
I am a beginner in FullPro, and now facing the problem of multi atom doping, how can I determine the doping position? Our current sample is doped with 3 atoms, and the doped element has 4 lattice...
19 February 2024 5,507 3 View
What does this error means in fullprof refinement process i.e. "Current parameters not saved to the current PCR file: final(Chi2) > 1.2*initial(Chi2) => Current parameters are saved in a...
12 February 2024 1,084 1 View