Hi, SEM sample preparation can be very different, from just taking (or cleaving) your sample to something more complex such as Au sputtering, sonication in solution, et cetera. If you could give some more information on your sample, I'll be more than happy to help if I have a similar experience.
thank you jea. but I'm SEM operator and i see diffrent samples everyday. i need a source about sample preparation for all kind of samples bulk material powder materal biomaterial and etc. i like to need more than usual sample preparation thank you again