What is the problem in attached file?

I have done ORR LSV (attached file) at different RPM (400-2000) in 0.1M KOH electrolyte (PH=13) using RDE. My teacher said that it is wrong due to limiting current density. Kindly give me your...

08 September 2019 1,662 2 View

How to do Particle Size Distribution of very small particles?

I used Image j but I didn't get correct result, is there another way to calculate particle size?

05 June 2019 8,862 3 View

What is the correct way of conversion of ppm to ppb?

Please suggest me a correct method of dilution of solutions to convert ppm to ppb. Let suppose I have 0.05 mg/ml solution, it has 50 ppm and I want to convert into different ppb solutions like 50,...

04 May 2019 9,307 1 View

How I can match simulated and own XRD pattern in Origin?

Hi, I have used American Mineralogist crystal database and downloaded .cif files and then used VESTA software to simulate XRD pattern and also have jcpdf number, I want to match with my own XRD...

04 May 2019 1,468 4 View

How can a beginner learn the analysis of X-ray photoelectron spectroscopy (XPS) by himself?

Is there any literature or trilaterals?

04 May 2019 3,309 6 View

Can anyone provide me JCPDS files?

Hi, everyone, I needed JCPDS files of Pt, Cu, PtCu & Cu3Pt, if anyone have then please share with me, I will be highly thankful. File numbers are as follows: PtCu = JCPDS 48-1549 Pt = JCPDS...

04 May 2019 1,856 4 View

What does it mean pass/fail in BET result?

I did BET for my catalyst (PtCu Nano particles) when I got result, I saw this error (given in attached figure), as BET Surface area is too low, what does "fail'' mean? is it incomplete analysis or...

03 April 2019 7,043 10 View

How can a beginner learn the analysis of XRD Powder method by himself?

Is there any literature or trilaterals?

01 February 2019 4,976 12 View

How to convert a potential collected with reference to Hg/HgO to Reversible Hydrogen Electrode?

I have collected a LSV data by taking Hg/HgO as the reference electrode. But I want to convert this one to RHE. Please suggest me the required conversion equation. 0.1M KOH was taken as the...

01 February 2019 6,730 4 View

Does anyone have the cif. file for ZIF-8 and MOF-74 ?

11 December 2018 8,137 0 View

Does the pressure(-600 mmHg) affects pH?

When I conducted the degassing experiment using decompression under anaerobic condition(and I used ferrous based chelating agent), the oxidized ferric were observerd. So, could you tell me the...

03 March 2021 4,892 5 View

Which database would give me this list of chemical components?

Dear colleagues: I would like to know if anyone knows of a database that gives me the parameters pH, K, K, Mg, P, C, N, Zn, Cu, Ni and Cd of common foods. I find a lot of information of proteins,...

26 February 2021 5,525 3 View

Why is NH4OH added in heavy metals limit test?

The limit test I'm referring to is USP method II. In this procedure you need to dropwise add 6N of NH4OH to the sample until it the pH is alkali. After that you need to dilute and add HOAc until...

23 February 2021 2,049 3 View

Is there an ideal incubation time of RGO-modified SPCE before subsequent use, i.e., electrochemical characterization or further modification?

I notice that upon washing and air-drying of my RGO/SPCE surface and characterizing again via DPV, the current response towards ferricyanide probe significantly decreases. My worry is that the...

22 February 2021 5,324 3 View

No title

22 February 2021 9,932 11 View

How to prepare electrolyte of NaClO4 salt for Na-ion battery? Any problem with this salt?

Hello, I am trying to make anode for Na-ion batteries. I have no experience with preparation of the electrolyte for any batteries. NaClO4 salt are available and I am planning to use EC:PC as...

21 February 2021 8,132 1 View

Can anyone help or comment on solubilising chlorobutanol in aqueous injections in minimum time possible?

Please suggest solubilisation of chlorobutanol in injections. Tried pH and high temperature. But the issue is of assay drop. If anyone can suggest any solution. Its a commonly used excipient for...

21 February 2021 7,397 1 View

What reaction will occur when adding hexamine into ammonium nitrate in an acidic medium?

Hello, I am investigating properties of water in oil emulsion explosives. And adding hexamine (hexamethylenetetramine) into one of the phases that are used to make the emulsion should increase the...

21 February 2021 8,680 1 View

What properties of water shall be analyzed and evaluated to test the effectiveness of activated carbon?

I would like to ask what other properties of water (pH and such) shall be analyzed and evaluated to test the effectiveness of activated carbon from filtering the contaminants present in the water?

20 February 2021 9,422 8 View

Phenol-pH graphic?

We want to use phenol pH graphic to measure the pH of mediums before and after inhibitor application to cells. We have phenol absorbence values at 460, 560 and 720 nm wavelength. When we measure...

20 February 2021 7,700 3 View