X Ray diffraction book by cullity. You can more information from this.

You can do XRD on some standard samples and analyse with some software's.

Hello,

I strongly recommend a book "X-Ray Diffraction A practical Approach" by C. Suryanarayana and M. Grant Norton, if you are looking for basic approach to analysis XRD. In this you will find many example which you have to solve for learning basic approach behind XRD analysis.

And also a book by Cullity for build up your concept.

P.S. I suggest you to go first with suryanaryana then after Cullity

Use Xpert High Score software to analyse your sample, tutorial for this you easily find at youtube.

Good Luck

Dear Anand,

I think for beginners it may be a little difficult to analyze the XRD data. But it is very simple. With more study and experience, you will be friendly with this powerful and most essential characteristics tool. I would like to suggest you to read some basic things which would be very helpful to you. Please follow the below link.

http://prism.mit.edu/xray/Introduction%20to%20XRPD%20Data%20Analysis.pdf

For analysis of XRD the most widely used procedure is,

1. 1st do the XRD and get the .txt, or .csv file and try to plot in Origin software

2. Next, try to find the JCPDS standard card number for your material [E.g. Magnetite nanoparticles (JCPDS card no. 00-001-1111)]

3. Try to match the peak position in your origin file and find the planes (hkl)

Please note this is very simple basic information to start with XRD. This is a very powerful tool to explore too many things you need to know.

Hope it helps you…

Thank you so much you all for your precious time and kind suggestions

Please refer book "X Ray diffraction" by B.D. Cullity.

Please search some vidoes in youtube also.

Please refer this article:

https://doi.org/10.1142/S0219581X04002620

Prediction of analysis, I have learned from you tube Video. you can also do the same

The texts listed by others are good. Cullity was used back in the 70s, but is still valid. Assume you have access to an X-ray diffractometer. Recommend you get some alumina (aluminum oxide) powder and generate a pattern. You'll need to learn about Bragg's law, and calulate d spacings. You'll need a catalog of materials/ d spacings you can get on the IN. It won't take you long to get the basics; but, the tool is much more powerful than for just material identification. Good luck. Learn by doing!

Thank you so much for your kind suggestions.

Just a remark:

The full text of the 'Cullity' reference mentioned some times above can be easily found by 'googling' for 'Cullity diffraction'......

I have downloaded above recommended books, thanks for you precious time and suggestions. Thanks again.

HI

The bigginar can be studied the basics of XRD by reading test book called Gluti. kindly check it.