Electrochemical exfoliation of graphite was done using graphite electrodes in an acidic condition. After that, washing and drying of graphene oxide were done. Thereafter, reduction of graphene oxide was done at 650 degC for 3 hours by using muffle furnace in Nitrogen atmosphere. We observed that the colour of the resultant reduced graphene oxide was milky white. Actually, it should be brown or black, I think. That's why we assumed that the process of reduction of graphene oxide failed. Therefore, please let me know why we failed that process and what was wrong with the process. Please let me have your advice, comments and suggestion. Thank you in advance.