I am looking at preparation of graphene oxide by microwave but when I used top and bottom, they break. Please help.
I suggest teflon reactors. They are commercially available together with microwave oven from: http://cem.com/en/mars-6/
Best regards,
Bartek
If you want to synthesize graphene in a commercial microwave oven, Teflon beakers are really good.
Conventional Microwave synthesizer are available in market for large scale production. Pl check it out.
http://cem.com/media/contenttype/media/literature/525_Broch_Inorganic_Synth_B076.pdf
Thank you so much Drs.
Well if your operational temp is below 325 C you can use teflon vessel. Its most commonly used and cheap. But for high temp operations you have to go for quartz vessel. Its more expensive though.
Sending some links. Hope that's helpful.
http://www.sineomicrowave.com/products.aspx?ProductsCateId=116&ProductsId=129&orderid=53
http://web2.uconn.edu/chemistry2/leadbeater/Equipment.html
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