I am analyzing some sample using a GC keeping oven, injector, FID temperatures about 350 oC, 370 oC and 380 oC respectively. Unfortunately, after each analysis, when the column oven reaches initial temperature (220 oC), the nuts used to tighten the capillary column at the injector and detector ports are getting loosened and causing leakage. How to solve this issue, suggestions please?!

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