Current I am using calcium hydroxide but at higher pH it make gel type material
Maybe this way. First, you would have to precipitate both sulfate out of solution. Then you would use the property that nickel sulphate (hexahydrate or heptahydrate) is soluble in ethanol but aluminum sulfate is insoluble in ethanol.
Nickel sulphate is insoluble in most of alcohols like ethanol and propanol
But hexahydrate or heptahydrate is soluble.
https://www.chemicalbook.com/ChemicalProductProperty_EN_cb7498462.htm
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Thanks
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