I'm trying to make an electrospinning sol-gel per a literature procedure, but the TTIP is precipitating to TiO2. In short, I am dissolving polyacrylonitrile into DMF at 80ºC, followed by dropwise addition of a TTIP/ethanol solution in N2 atmosphere. The TTIP is instantly forming a precipitate when it encounters the PAN/DMF solution. Any advice?

http://pubs.rsc.org/en/Content/ArticleLanding/2012/JM/C2JM14852H#!divAbstract

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