Why size of the quantum dots increased after attachment on the glassy carbon electrode surface?

Size of the quantum dots is 2.3 nm after attachment on glassy carbon substrate, the size drastically increased to 40 nm. but shape of the Quantum dots is retained. is it due to aggregation?...

02 March 2019 1,954 3 View

Is it possible to get high electrocatalytic activity with electrode with lower electroactive surface area?

is it possible to get high electrocatalytic activity with electrode with lower electroactive surface area? what are the factors affecting electrocatalytic activity of the modified electrodes?

05 June 2018 6,355 0 View

Is it possible C-O bond formation like C-N bond in glassy carbon electrode in the basic condition?

is it possible C-O bond formation like C-N bond in glassy carbon electrode in the basic condition? In alkaline condition is Carbon-Oxygen bond formation possible in glassy carbon electrode?

31 December 2017 1,022 0 View

How to elucidate the structure of carbon dots?

How to find the exact structrue of carbon dots? i want to find the structure of carbon dots precursor for carbon dots was glucose is there any relation between precursor and structure of Carbon...

09 October 2017 8,077 1 View

Doubt in BSA capped Nanoparticles?

05 June 2017 6,152 3 View

How to remove Gold nanoparticles from glassy carbon electrode surface?

04 May 2017 5,962 7 View

Role of laviron equation electrochemical determination of methyl parathion?

04 May 2017 4,375 0 View

Is there any relation between pH and surface area?

02 March 2017 8,256 0 View

Can anyone suggest me negative redox potential biomolecules ?

please help to fine negative redox potential biomolecules like Hydrogen peroxide

01 February 2017 3,076 0 View

How to find the concentration of carbon dots?

How to find the concentration of Carbon dots? from weight of the starting materials how to find the concentration of carbon dots. is there any relation between the total weight of the starting...

31 December 2016 2,820 1 View

Why can't make aluminum nitride film successfully by use sputter?

We use reactive sputtering process to make aluminum nitride film, and want to make c-axis aluminum nitride film on a silicon substrate, but the crystal orientation cannot be seen with...

03 March 2021 7,975 3 View

What are the new 2D nanomaterials were used for Silver nanoparticles stabilization?

In the stabilization of AgNPs are vital in current research interest. However, some of the 2D nano-materials like graphene oxide, MoS2, etc... previously used to stabilize it. But still they shown...

01 March 2021 2,207 3 View

How does charge on working electrode changes with rising potential?

During performing CV of a GCE or modified GCE, we rise the potential in the first half of the cycle and reduce it in reverse half. During the first half, what is the nature of charge on GCE or...

25 February 2021 7,994 3 View

How to delaminate copper in water-based anodes?

Hello everyone, I'm looking for a way to delaminate copper current collector of water-based anodes in Li-ion batteries without damaging the graphite film. I tried different materials such as HNO3...

24 February 2021 3,785 3 View

Thermal reduction of graphene oxide.?

I am trying to reduce graphene oxide by thermally but I have no proper information regarding this. Can any one help me regarding the details about temperature and time for the reduction of...

23 February 2021 4,155 4 View

What kind of steel moulds are used for hot pressing metal powders?

My main concern is that the metal powders should not weld to the mold surface and I should easily be able to eject out the pressed samples. I am looking for alternative for graphite moulds. The...

22 February 2021 2,965 4 View

Is there an ideal incubation time of RGO-modified SPCE before subsequent use, i.e., electrochemical characterization or further modification?

I notice that upon washing and air-drying of my RGO/SPCE surface and characterizing again via DPV, the current response towards ferricyanide probe significantly decreases. My worry is that the...

22 February 2021 5,324 3 View

How to Study a proton NMR of Graphene prepared by Electrochemical Exfoliation technique?

I performed a Proton NMR of graphene powder prepared by electrochemical exfoliation technique. It shows some peaks. But I can't understand it.

21 February 2021 8,947 3 View

Which compound is getting oxidized during bulk electrolysis with TFAA?

The experiment is really simple. When I do a bulk electrolysis with 1% TFAA (ACN solution) to get dihydrogen, what is going to be oxidized? (working electrode graphit, counter electrode platinum,...

18 February 2021 4,430 1 View

Mixture neutralization after Boc deprotection ?

I am performing a Boc-deprotection with HCl in organic solvent (dioxane or Ethylacetate) but would like to isolate the free amine. Several problems: - Neutralizing with inorganic base as NEt3...

18 February 2021 3,366 3 View