Hello, if you have a recent version of Topspin you can simply type "rpar B11ZG" and it will load a standard Boron-11 parameter set. If you do not have such a parameterset just use edasp to choose B11 as the observe nucleus. An easy first sample to measure is NaBH4 in D2O. It will appear at ca -42 ppm as a pentet ( 5 lines). The lines are sharp. You can use your 13C pulse and power as a starting value.