28 December 2019 0 7K Report

I'm plating copper with nickel (electroless). Then, I'm doing porosity test according to the procedure below. I can't find the exact reactions going on between the ferrocyanide and the copper electrode beneath the nickel plating.

I've found a reaction with copper ions, but I don't understand how it reacts with solid copper (or how copper ions are formed).

2Cu+2(aq)+[Fe(CN)6]4−(aq)↽−−⇀Cu2[Fe(CN)6](s)

thank you in advance!

Porosity test procedure:

  • Prepare the porosity bath as described in the procedure.
  • Place double sheet of paper on the table.
  • Place two glass slides on top of the paper.
  • Put filter paper on each slide.
  • Put some of the porosity solution on top of one filter paper with plastic pipette.
  • Place your electrode on the wet filter paper, and then pour some more porosity solution on top of the electrode.
  • Place the other filter paper on top, make sure it is wet (if not add some more solution).
  • Place the second glass slide on the top and wait 20 minutes.
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