We want to prepare graphene or reduced graphene oxide. I am looking for a technique that can produce graphene directly onto glass substrates. Can anyone let me know which method is best. Any references?
Following articles will help you
1) Synthesis of Graphene and Its Applications: A Review
http://www.tandfonline.com/doi/abs/10.1080/10408430903505036#.Uvo1k_mSyao
2)Graphene and Graphene Oxide: Synthesis, Properties, and Applications
http://onlinelibrary.wiley.com/doi/10.1002/adma.201001068/full
3) Improved Synthesis of Graphene Oxide
http://pubs.acs.org/doi/abs/10.1021/nn1006368
4) Facile Synthesis and Characterization of Graphene Nanosheets
http://pubs.acs.org/doi/abs/10.1021/jp710931h
5) Functional Graphene Oxide as a Nanocarrier for Controlled Loading and Targeted Delivery of Mixed Anticancer Drugs
http://onlinelibrary.wiley.com/doi/10.1002/smll.200901680/full
Thank Rajashekar,
I have come across this method but not getting any reference book. Do you have any book related to it?
Fabrication of highly conducting and transparent graphene films
2.2. Preparation of graphene films on quartz substrates
http://image.sciencenet.cn/olddata/kexue.com.cn/upload/blog/file/2010/10/20101011233835521584.pdf
Following articles will help you
1) Synthesis of Graphene and Its Applications: A Review
http://www.tandfonline.com/doi/abs/10.1080/10408430903505036#.Uvo1k_mSyao
2)Graphene and Graphene Oxide: Synthesis, Properties, and Applications
http://onlinelibrary.wiley.com/doi/10.1002/adma.201001068/full
3) Improved Synthesis of Graphene Oxide
http://pubs.acs.org/doi/abs/10.1021/nn1006368
4) Facile Synthesis and Characterization of Graphene Nanosheets
http://pubs.acs.org/doi/abs/10.1021/jp710931h
5) Functional Graphene Oxide as a Nanocarrier for Controlled Loading and Targeted Delivery of Mixed Anticancer Drugs
http://onlinelibrary.wiley.com/doi/10.1002/smll.200901680/full
Not directly but after you synthesize GO from Hummers you can deposit GO films onto quartz or glass or silicon substrates by modifying them with a 1% APTES solution in 4:1 acetone/water solvent. Then, you incubate a GO solution about 0.5 mg/ml onto the modified substrate and wait to get your film. Then you reduce your GO film to rGO with hidrazine vapour (use a closed glass chamber with substrate facing up) and there you have rGo or GO films. All the references you get from the collegues are very useful indeed.
I hope the above specified articles will be good enough to decide the best approach of graphene preparation. However, you can try with the simple chemical method in presence of base, like KOH or NaOH under microwave irradiation will help you to get defect free graphene sheets. Also, you refer this article..
Good luck
You can try with modified Hummer's method or chemical vapor deposition method. You can find many papers related graphene synthesis.
Dear researchers
What is the best method to have following advantages:
1- high yield and pure and homogen (size, functional groups in both sides ) GO structures
2- well disperesd in water , stable over some time
3- single layer and have large lateral dimension (micro meter)
4- easy to perform in ordinary lab.
5- proved and cited in other works
Regards
Which method is good for high yield for Graphene Oxide preparation ? - ResearchGate. Available from: https://www.researchgate.net/post/Which_method_is_good_for_high_yield_for_Graphene_Oxide_preparation#58a9a4cbeeae396e527216f6 [accessed Feb 19, 2017].
Very easy way for high quality Graphene Oxide synthesis,
http://instanano.com/nanomaterial-synthesis/carbon-nanomaterial/easy-synthesis-of-high-quality-graphene-oxide-new-method/
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