After extraction in n-hexane and removing thiocompound with copper powder you can inject in GC-MS for separation and identification of phenolic compounds
The best method to extract polyphenols is to make a liquid-liquid extraction, ie the Amount of 100 g of vegetable filtered through a Whatman filter paper No.1
Were delipidated by 29 100 mL of hexane. The delipidated OMW Was Then
Extracted with 29 100 mL of ethyl acetate. The organic phase of WAS dried over 3 g of
anhydrous sodium sulfate and Then using a rotary evaporator Concentrated set at