I want to know how to find the %crystallinity from PXRD peaks. I have a highly amorphous compound where I get a broad peak. For your reference my PXRD looks same as in the following picture.
You can perform XRD deconvolution using software like Origin to get broad as well as crystalline peaks. Find the area under crystalline peaks (Ac) and also total area (At). Divide Ac by At and multiply by 100 to get the degree of crystallinity