I am preparing the GO nanosheets using Hummer's process, but synthesized nanosheets are of very high polydispersity in terms of lateral dimensions. Is there any method by which the polydispersity can be minimized?
You can try ultra-sonication during reactions. this will help to decrease aggregation... In a different way, you can also try to reduce the reaction rate by lowering the temp during reactions. you can try making the reaction in a ice bath under ultra-sonication. Some particles will be large still. Use centrifugation at the end to remove larger particles..