Hello! Can someone guide me please about following description?

20 February 2019 1 352 Report

I am labelling my peptide with MW 768.46 with FITC in DMF/TFA/H2O solvent mixture. After 12 hours stirring i get my product. It is a liquid mixture, i want to get solid product. Which method is suitable to get solid product? Or can i add some solvent which can produce precipitates of my product and I get solid product by paper filtration. Please reply me ASAP.

Thanks in Advance!

Jai Ghosh

I think it would be better to check if you can get the solid product by reducing its solubility either by increasing the dipole moment of the solution or by reducing its dipole moment.

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