let me know your sample matrix. because extraction procedure is deference for the sample matrix.
hoe ever, Method given below is most suitable for both quantification and identification.
ASTM D7065 – 11 ( Standard Test Method for Determination of Nonylphenol, Bisphenol A, p-tert -Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol Diethoxylate in Environmental Waters by Gas Chromatography Mass Spectrometry)
However, if you don’t have that GC/MS facility, you can use HPLC with florescent detector attached herewith for your analysis. Also, aging, you have to select suitable extraction procedures for your sample matrix. Further, you have to use another analytically technique for the confirmation.
You can use HPLC-UV with a C18 column, an injection volume of 20µL. The mobile phase is Methanol/Water 70/30 and the flow is 1mL/min. Bisphenol can be dissolved in methanol.