Different Raman spectra of graphene like quantum dots?

The characteristic raman spectra that I've obtained for graphene like quantum dots shows a kink at about 1450 cm-1, this is different from the reported literature. What can be the posible reason...

01 February 2020 2,243 3 View

How can I index XRD peaks of a graphite like sample?

I've a nano-scaled graphite like material, the XRD pattern is showing some peaks which are not matching with any of the reported literature. For example usually a broad peak is seen around 21...

01 February 2020 6,185 2 View

What can be the perfect GC-MS operating conditions for acetonitrile?

I have to analyse the change in composition of acetonitrile after being reacted mechanically at different time intervals, hence I'm planning to undertake a GC-MS of the samples. Can anyone suggest...

05 June 2019 9,128 8 View

What is a Solid State Metathetic Reaction?

What kind of synthesis is this SSM route useful for?

03 April 2018 9,998 2 View

Can retention time for a particular compound change when detected at various wavelengths?

I'm using a PDA detector HPLC unit, I was wondering whether it is possible that the retention time can change for a particular compound when the detector is set at a different wavelength, all...

11 December 2017 5,337 6 View

What can be the plausible reason for increase in the area of a peak in HPLC spectrum, even when the reaction is to degrade the compound?

I'm withdrawing samples after a 15 minute interval for 90 minutes. Hence, the 90th minute sample is to show the highest amount of degradation or the least peak area, but it shows the highest, this...

10 November 2017 5,853 7 View

Why is the lambda max of dibenzothiophene chosen as 275-284nm and not 230-240nm?

In most research papers the wavelength chosen for DBT detection is 284nm, but according to the NIST data the maximum absorbance occurs around 230-240nm. Can anyone explain why it is...

07 August 2017 3,923 4 View

What could be the HPLC conditions for thianaphthene/benzothiophene?

07 August 2017 8,177 4 View

Which is the better analytical software Modde Pro or Design expert? Why?

07 August 2017 5,576 4 View

Will dextran coated iron oxide nano particles react adversely in an acidic medium?

Nanoparticles Iron oxide Acid HCl coating

05 June 2017 7,300 4 View

After a reference from Int J Body Compos Res, can any body help?

Hi, I am after the reference below, my library says it cannot obtain a copy either locally or internationally, any help appreciated! Chris Wang ZM, Heshka S, Wielopolski L, Pi-Sunyer FX, Pierson...

03 March 2021 6,193 1 View

Can we block unwanted images during the x-ray prediction?

i am try to classify the x-ray images. During classification , can i block unwanted images (except x-ray image).

03 March 2021 7,100 1 View

Why Austenite grains in steel show much more twinning than ferrite grains?

It is oftentimes said to be a distinctive metallographic trait that differentiates a fully austenitic and a fully felly ferritic steel without etching that might distinguish between two. Why...

02 March 2021 728 2 View

Does anyone know to clarify these changes?

01 March 2021 1,290 2 View

In an eye with Tyndall, does each dot correspond to an individual cell?

When you observe the presence of Tyndall in an inflamed eye: Does each of the small floating dots correspond to an individual cell or to an aggregate of cells? Does a conventional slit lamp have...

27 February 2021 6,326 2 View

How to calculate the crystallinity of cellulose film?

27 February 2021 2,753 4 View

What could be the reason for not having further low chi square value (better agreement) in my refinement result?

I have tried every combination of parameter changes and after that i have a poor chi square value. I can't get it lower any further. I know there have been a lot of discussion about Rietveld...

26 February 2021 8,480 3 View

Can anyone share his experience regards Smoothing in origin?

I am working on TiO2 composite material and the results of XRD have a lot of small/junk peaks and while I apply a smooth filter in Origin then the other characteristics peaks disappear so anyone...

26 February 2021 8,183 3 View

How to replicate the well conditions of a crystal hit with 20%(w/v) isopropanol?

I had a crystal hit in a well with 0.1M HEPEs pH 7.5, 10%(w/v) PEG 4000, and 20%(w/v) isopropanol. Why is isopropanol in w/v here if it's just solvent? How do I recreate this well condition?

25 February 2021 9,761 1 View

I have need of XRD graph analysis software for phase identification. Can you please provide links for software tools which can be downloaded?

i am trying to download x'pert high score software, but can't download it. please do suggest software for phase analysis

24 February 2021 5,687 4 View