From powder XRD we can measure the value of basal spacing. The value of basal spacing should be increased for the intercalation process. So, for liquid samples is this theory applicable or not?
Please look at the attached paper
If you optimize the concentration of the phase of interest ant using a blank of the solvent, you could use SAXS technique to measure basal spacings.
Require for Rietveld refinement in XRD.
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