I want to make a Teflon reactor , with quartz window for Photo-electrochemical characterization having three electrodes . I need help in making can some show me the photo or the sketch how to make it .
TO KNOW MORE ABOUT MY QUERY read the " section 2.3 " as ------
The PEC experiments were performed in a Teflon reactor equipped with a quartz window for frontal illumination. All the tests were carried out in a three electrode configuration using the TiO2 NP film, TiO2 NTs, ZnO NWs or ZnO@TiO2 core– shell heterostructures as the working electrodes for the water photo-electrolysis reaction, a platinum wire as the counter electrode, and an Ag/AgCl (KCl 3 M) as the reference electrode, in a 0.1 M NaOH aqueous electrolyte (pH = 12.7).
here i got no idea what the reactor is . and i need to make it .. help me in making it .
It's not a good idea to use Teflon in studying water splitting. Teflon is a gas permeable material. You will always have a contamination of the head space with O2, which is a real problem for both water oxidation and reactions
Yurii V Geletii sir what material should i use and how ? any sketch or pic
See SI in
Article Stabilization of Polyoxometalate Water Oxidation Catalysts o...
I think using Ag/AgCl at 12.7 mean alkaline medium is not a good choice. But if some senior could suggest/correct me I will be grateful. Thank you
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