I want to quantify phenolics present in my aq. methanol extract using gc ms. But i want to make the extaract volatile so that it could separate out the phenolics. Please guide me to prepare my extract as such in easy way.
Dear Negi, check this article. might be it can help you in the preparation of sample for GC-MS.
Try one of these methods
https://www.sciencedirect.com/science/article/pii/S0308814605000294
Article Development and validation of a GC/MS method for determinati...
Article Separation, Characterization, and Quantitation of Benzoic an...
Dear Negi, please find attached file for kind information this will be heplpfual for you.
Good Luck!
Negi look though these papers.
cheer!
https://www.mdpi.com/1420-3049/18/2/2328/pdf
http://www.mdpi.com:8080/2304-8158/2/1/90/pdf
http://web.chemistry.gatech.edu/class/analyt/gc.pdf
Article Analysis of Phenolic and Cyclic Compounds in Plants Using De...
https://link.springer.com/article/10.1007/s11434-010-4266-1
Article GC-MS Determination of Flavonoids and Phenolic and Benzoic A...
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