I am having trouble performing pulse calibration on TPR equipment. I used the pulse calibration function indicated by the equipment, however, I can't perform the analysis; a message saying that argon should be the first analysis gas appeared. I already tried changing the gas inlets, but it didn't work (I've also tried modifying the absorber gas and carrier gas in the method). I have no idea how to solve this problem and the manual does not provide details about this. If anyone can help me and have information on this subject I would appreciate it.
It's possible that the pulse calibration function in your TPR equipment is specifically designed to work with argon as the first analysis gas. It could be that the method or configuration you are using is not compatible with the pulse calibration function. To solve this problem, you may try to run the pulse calibration function with argon as the first analysis gas, as indicated by the message. If that does not work, try contacting the manufacturer.
I appreciate the answer. I have already performed tests using argon as the first gas, and a message appears saying that the H2/Argon mixture must be the first gas. I am using argon in the pulse gas line and the H2/Ar mixture in the first inlet (inlet 101). I have already performed tests using argon on line 101 and the H2/Ar mixture on line 102. However, none of the alternatives worked.
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