How do we treat zero values in a time series before running Holt Winters Multiplicative model?

I want to understand the functioning of a tool. I've been told that the tool performs multiplicative decomposition of the time series before forecasting. I've managed to decompose the series in R...

02 March 2019 3,430 4 View

I need images of machine parts (automotive industry) to perform damaged parts detection. Please help!!?

Aim is damaged part detection (i.e. scratch, dent, holes, pits, etc.): e.g. Automotive/Industrial part stamping quality inspection, Rolled sheet metal surface inspection, Pit/hole detection in...

04 May 2018 9,257 1 View

Why are graphite-acid intercalation compounds preferred for preparation of exfoliated graphite?

Graphite can be intercalated with a number of compounds including halides, alkali metals, halogens etc. Yet most of the literature points towards use of graphite-acid intercalated compounds.

05 June 2017 8,491 0 View

How does degree of intercalation depend on graphite particle size in liquid intercalation (H2SO4-HNO3)? Can oxidation occur in very fine particles?

I wish to intercalate very fine graphite particles through a mixture of concentrated H2SO4 and HNO3. Normally, small particle size results in greater degree of intercalation. Is it possible for...

04 May 2017 2,747 2 View

Can I perform an electrochemical reaction in parts?

I have a reaction which will most likely take around 10 full days to finish. Since the equipment in my lab can not run for so long continuously, I was wondering if I could perform the reaction in...

02 March 2017 4,671 2 View

Can I use a muffle furnace instead of microwave irradiation for preparation of expandable graphite?

I am trying to prepare expanded graphite. During literature review, I came across heat treatment, ultrasonic irradiation and microwave irradiation as methods of expansion after intercalation. Due...

08 September 2016 6,408 7 View

Calculate value of 'c' parameter for intercalated graphite using XRD data?

01 January 1970 750 4 View

How to prepare graphite electrode from graphite powder, to be used in in electrochemical reaction using aqueous and concentrated H2SO4 electrolytes?

01 January 1970 7,171 3 View

Could you help me with some basic concerns regarding graphite expansion?

Hey there! I am working on non-oxidative intercalation and expansion of graphite using sulfuric acid. I've investigated both electrochemical and liquid intercalation methods using 2*2 cm of...

01 January 1970 8,522 1 View

How to perform XRD of very small graphite sheet sample?

I have a very small sample of graphite sheet (10mg, 36mm2) of which I need to perform XRD. The detected area of the instrument I am using is 6.25cm2. How can I perform XRD of such small sample?...

01 January 1970 5,594 3 View

What are the new 2D nanomaterials were used for Silver nanoparticles stabilization?

In the stabilization of AgNPs are vital in current research interest. However, some of the 2D nano-materials like graphene oxide, MoS2, etc... previously used to stabilize it. But still they shown...

01 March 2021 2,207 3 View

How does charge on working electrode changes with rising potential?

During performing CV of a GCE or modified GCE, we rise the potential in the first half of the cycle and reduce it in reverse half. During the first half, what is the nature of charge on GCE or...

25 February 2021 7,994 3 View

How to delaminate copper in water-based anodes?

Hello everyone, I'm looking for a way to delaminate copper current collector of water-based anodes in Li-ion batteries without damaging the graphite film. I tried different materials such as HNO3...

24 February 2021 3,785 3 View

Thermal reduction of graphene oxide.?

I am trying to reduce graphene oxide by thermally but I have no proper information regarding this. Can any one help me regarding the details about temperature and time for the reduction of...

23 February 2021 4,155 4 View

What kind of steel moulds are used for hot pressing metal powders?

My main concern is that the metal powders should not weld to the mold surface and I should easily be able to eject out the pressed samples. I am looking for alternative for graphite moulds. The...

22 February 2021 2,965 4 View

How to Study a proton NMR of Graphene prepared by Electrochemical Exfoliation technique?

I performed a Proton NMR of graphene powder prepared by electrochemical exfoliation technique. It shows some peaks. But I can't understand it.

21 February 2021 8,947 3 View

Which compound is getting oxidized during bulk electrolysis with TFAA?

The experiment is really simple. When I do a bulk electrolysis with 1% TFAA (ACN solution) to get dihydrogen, what is going to be oxidized? (working electrode graphit, counter electrode platinum,...

18 February 2021 4,430 1 View

What is the best substrate for exfoliating few layers of hexagonal boron nitride (hBN) using traditional scotch tape method?

Unlike graphene, it is usually very difficult to exfoliate few layers (~10 nm thick) of hBN on SiO2 substrate due to lip-lip interaction at the edges. Au substrates have been proven very useful...

16 February 2021 2,635 2 View

About XRD details of pristine and doped RGO?

Hi Can anyone please help me know the XRD details of reduced graphene oxide, Nitrogen doped reduced graphene oxide, Sulphur doped reduced graphene oxide, Nitrogen and Sulphur co-doped reduced...

08 February 2021 3,033 3 View

What is the difference between Graphene Oxide and Expanded Graphite?

What are the main differences between Graphene Oxide and Expanded graphite, in terms of surface functionalities, conductivity, d-spacing and other features? Is the term expanded graphite...

06 February 2021 9,810 4 View