I synthesized PEDOT through electropolymerzaition in 10% acetonitrile (v/v) and deionized water in the presence of LiClO4 and of course the monomer EDOT.

The reference electrode used is Ag/AgCl, the counter electrode was glassy carbon and for the working electrode (where the PEDOT was formed) i used a graphite sheet. The scan rate is 100mV/s.

I attached the pictures of the voltammograms as well as the electropolymerized PEDOT on the graphite sheet.

Thanks

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