I am trying to deposit PB on carbon electrodes.
I tried electrochemical deposition. I couldn't deposit any thing, I did chemical synthesis and dropcasting on the surface of the electrode. looks like it is too thick and i see the electrode response, not a gradient. just the height of transition current is changing when i change the analyte concentration. any ideas how to handle it?
Dear Ameneh Mohammadnezhad,
electrodeposition depends essentially on the value of the potential to be imposed on your electrode. I'd like to know how and on what basis you took this value of E?
cordially.
Naima Ghemmit-Doulache
I did Galvanostatic deposition according to this paper: Article Electrochemical Behavior of Electrodeposited Prussian Blue F...
I also did a cv in the same bath from -0.2 to 0.6
neither worked. I didn't try potentiostatic deposition.
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