Which steps, materials, temperature or stirring contain this process? Is there any publish or book? I want to materials make up only sulphuric acid and pyrrole monomer. Because my materials are unsufficient.. Thank you for your attention.
Alvena Shahid
In 100 milliliters of pure water, dissolve 0.1 mol of pyrrole monomer. After adding 0.1 mol of sulfuric acid, give the mixture ten minutes of stirring. Stir the mixture for an additional ten minutes after adding ten grams of graphite powder. The mixture should be transferred to a glass beaker and left in a water bath at 60°C for a full day. After filtering the solid product, repeatedly wash it with distilled water. For 12 hours, the product is dried in an oven set at 80°C.
Method:
This procedure and its applications are covered in a few books and publications, including:
- Wan, C., Chen, X., & Liu, X. (2021). Synthesis and Mechanism of Spherical Ag-doped Polypyrrole Assisted by Complexing Agents. Journal of Inorganic and Organometallic Polymers and Materials, 31, 4463-4472.
- Chemical synthesis of polypyrrole doped with dodecyl benzene sulfonic acid Vol4_Issue1_08.pdf (jsirjournal.com)
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