I have performed cyclic voltammetry for electro-oxidation of methanol using nanoparticles modified GCE.
I need to calculate the ESA for modified GCE?
Please suggest me for the same.
Thanks
what material are you modifying your GCE with?
It appears that for palladium the oxide reduction peak is used to determine the ESA.
You need to measure the charge of the reduction peak and normalize it by mono-layer charge and weight of the palladium.
@Fernando..
The GCE was modified by 10 microleter of N-rGO/MnO2 composite (5mg/mL).
i am unable to interpret why its increases in start as shown in figure
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