How to confirm the phase transition from R3c to orthorhombic?

Indoors BiFeO3 has r3c st and with doping it goes to orthorhombic. But the exact orthorhombic structure group is not clear.which is correct r3c to pbnm or r3c to c222. How to check it appropriately.

11 December 2018 8,917 3 View

Anyone here using PE loop tracer system from Marine India?

Please inbox me. I have some queries regarding the instrument. Thank you in advance. Regards Alaka

10 November 2018 4,602 0 View

Can anyone suggest me if the attached result signifies the ferroelectric behaviour ?

I am herewith attaching the PE result (ferroelectric hysteresis) with finite loop area. I need suggestions regarding following 1. As can be seen the loop ahifted to left from origin and some cases...

31 December 2017 9,127 9 View

What is the effect of electrode on the polarization-elelctric field loop (PE loop)?

07 August 2017 4,846 0 View

What will be the effect of impurity on Dielectric properties of semiconductor?

How does the morphology of impurity affects the dielectric properties. The impurity phase is Hematite so can anyone suggest or refer some literature regarding this.

05 June 2017 8,409 8 View

What does it mean when Zero field cooled (ZFC) and field cooled (FC) curve completely merge with each other?

what does the peak observed in ZFC and FC imply? how does it related to spin glass transition? How to confirm the same? Can anyone please suggest me.

05 June 2017 1,413 4 View

Does increase in peak shifting with higher 2 theta angle in XRD logical?

I am observing the shift in peaks in a mixed phase system (2 phases). I observed the peak shifting is more at higher angles i.e if it is 0.2 upto 2 theta =30 degrees which increases to 0.4 towards...

05 June 2017 5,782 16 View

What does the enhancement of intensity of certain peaks in XRD pattern implies?

I am working on Bi2Fe4O9 sample which shows some planes getting enhanced after sintering. The specific planes are (001),(002),(140). Can anyone suggest what it is due to?

04 May 2017 5,684 5 View

Can I use any matrix for PE loop measurement?

31 December 2016 7,891 6 View

Can anyone help me out on analysis of PE loop?

31 December 2016 8,288 0 View

After a reference from Int J Body Compos Res, can any body help?

Hi, I am after the reference below, my library says it cannot obtain a copy either locally or internationally, any help appreciated! Chris Wang ZM, Heshka S, Wielopolski L, Pi-Sunyer FX, Pierson...

03 March 2021 6,193 1 View

Can we block unwanted images during the x-ray prediction?

i am try to classify the x-ray images. During classification , can i block unwanted images (except x-ray image).

03 March 2021 7,100 1 View

Does anyone know to clarify these changes?

01 March 2021 1,290 2 View

In an eye with Tyndall, does each dot correspond to an individual cell?

When you observe the presence of Tyndall in an inflamed eye: Does each of the small floating dots correspond to an individual cell or to an aggregate of cells? Does a conventional slit lamp have...

27 February 2021 6,326 2 View

How to calculate the crystallinity of cellulose film?

27 February 2021 2,753 4 View

What could be the reason for not having further low chi square value (better agreement) in my refinement result?

I have tried every combination of parameter changes and after that i have a poor chi square value. I can't get it lower any further. I know there have been a lot of discussion about Rietveld...

26 February 2021 8,480 3 View

Can anyone share his experience regards Smoothing in origin?

I am working on TiO2 composite material and the results of XRD have a lot of small/junk peaks and while I apply a smooth filter in Origin then the other characteristics peaks disappear so anyone...

26 February 2021 8,183 3 View

How to replicate the well conditions of a crystal hit with 20%(w/v) isopropanol?

I had a crystal hit in a well with 0.1M HEPEs pH 7.5, 10%(w/v) PEG 4000, and 20%(w/v) isopropanol. Why is isopropanol in w/v here if it's just solvent? How do I recreate this well condition?

25 February 2021 9,761 1 View

I have need of XRD graph analysis software for phase identification. Can you please provide links for software tools which can be downloaded?

i am trying to download x'pert high score software, but can't download it. please do suggest software for phase analysis

24 February 2021 5,687 4 View

Why the CHi^2 is close to zero with a bad fitting but the Rp and Rwp are still high?

I am refining my XRD data using in FullProf program. The intensity of the modulated X-ray peaks is almost flat. I tried to adjust the peak intensities but unsuccessful. What is the reason? I guess...

23 February 2021 2,304 4 View