i need to buy one teflon lined autoclave for my synthesis process. pressure is very important for finding a suitable autoclave among different models. is there any way i can calculate pressure of autoclave in synthesis process.
i use 0.75 g ferrocene as precursor and 75 mL aceton as solvent
You can calculate the "approximate" vapor pressure using Antoine Equation:
log10(P) = A − (B / (T + C))
P = vapor pressure (bar)
T = temperature (K)
Temperature range (K) :259.16 - 507.60
A 4.42448
B 1312.253
C -32.445
Reference :
https://dx.doi.org/10.1016/0021-9614(74)90119-0
https://www.researchgate.net/post/How_to_calculate_the_amount_of_pressure_created_within_the_autoclave_during_hydrothermal_synthesis
http://ddbonline.ddbst.com/AntoineCalculation/AntoineCalculationCGI.exe?component=Water
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