I'm making a boron-containing by-product which in only soluble in DMSO. I've been trying to make a crystal of that. I'm kind of sure is meta boric acid and I have a peak at around 20 ppm in B NMR.
You can find information on this topic in:
J.A. Peters, Interactions between boric acid derivatives and saccharides in aqueous media; structures and stabilities of resulting esters
Coord. Chem. Rev. 268 (2014) 1–22. DOI: 10.1016/j.ccr.2014.01.016.
In Section 3 (Interactions between bor(on)ic acids and simple inorganic anions), self-association of borc acid is reviewed.
Mahshid,
This is about right, from my experience the signal of boric acid in dmso-D6 appears as a relatively broad singlet at 19.9 pm in 11B NMR.
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