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I've been working on a new methodology for the synthesis of Triazene (N=N-NH). As long as I use deuterated acetone, I can take a beautiful NMR whereas using CDCl3 gives me a messy NMR for the same...
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I'm making a boron-containing by-product which in only soluble in DMSO. I've been trying to make a crystal of that. I'm kind of sure is meta boric acid and I have a peak at around 20 ppm in B NMR.
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