Don't know your matrix, but pls check Biomed Chromatogr. 1987;2(5):216-20; J. Chromatogr B Analyt Technol Biomed Life Sci. 2006 Oct 20;843(1):57-62. Good luck!
Cysteamine can probably be directly determined by acidimetric titration both in aqeous (by HCl or H2SO4) or nonaqueous (by HClO4) conditions. Titration is the best way if you have no reference. Find some advices and protocol here: