IS anyone familiar with encapsulation of materials in the food industry? I want to encapsulate a water soluble polyphenol with hydrogenated oil by simple hot-melt method. I am also required to determine the encapsulation efficiency. Evaluating the surface phenol and total phenol was the method i used. I tried washing the matrix with water and evaluating the conc. of surface phenol but the oil seems to be contaminating the water fraction thereby exaggerating my results. I though water, being miscible with oil would work. Anybody to help?