I am trying to remove the backside layer of CVD graphene from Cu foil using oxygen plasma etching. I am using the following etching conditions:

  • Initial base pressure ~0.16 mbar
  • Oxygen process pressure ~0.44 mbar (~40 sccm)
  • RF power: 75W
  • Etching duration: 30s
  • Sample size: ~1cm by 1cm

After etching for just 30s, the sample was very obviously burned. Would anyone know what the reason for this could be?

For background context, my CVD graphene product is more than 6 months old. The backside appears to be oxidised (see attached photo) due to exposure to air over time - could this be the reason why my samples are burning unexpectedly?

Thanks in advance.

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