Normally, the base catalyst complete its reactions within 1 hour where as the acid catalyst tends to finish within 2 hours during transesterification. What mechanism makes the base catalysts react faster than solid acid catalyst ?
I have electrospun pure ABS solution and measured the diameter and it was measured as 500s nm averagely. But surprisingly the fiber diameter decreases to 100s nm averagely while loading of MWCNT....
08 September 2018 2,628 1 View
we have light scattering instrument of Malvern Nano ZS series. I need to do a studies on change in Molecular weight of the sample. But im unable to perform it. I have seen a drop down menu in the...
05 June 2018 7,736 0 View
We have Malvern DLS Zetasizer instrument in our lab. I need to determine the size analysis by DLS method. I need to input the properties like RI and absorption Coeff of the material. Is there any...
09 October 2017 2,596 0 View
I have collected some waste cooking oil from hotels and it contains lots of left over fried items and loaded with carbon (black soot). I have to use it for my research work but finding hard in...
08 September 2017 6,210 0 View
After a novel synthesis method of a compound, I have found it as layered structure when I observed in SEM. This material was not having the layer structure before synthesizing it with the novel...
07 August 2017 5,058 5 View
I'm trying to impregnate the nanoparticles in micron size powder. Firstly I was trying with wet impregnation method. I guess the proper doping is not happening. Will hydrothermal or solvothermal...
05 June 2017 3,766 0 View
i have synthesised magnetic material Fe3O4 by co-ppt method. Before calcination, the magnetic property was showing but after calcination above 500 degree C , the magnetic property is losing....
01 February 2017 5,302 6 View
I'm trying to coat the Cerium Zirconium oxide NPs on copper tube. I have tried brush coating and dipped coating but its not sticking on the copper tube. Any suggestion for better coating, Please...
31 December 2016 9,019 1 View
31 December 2016 6,339 1 View
if anyone here read the paper about eggshell and reported the SEM image as flower-like structure then please let me know the name of the paper.
31 December 2016 7,772 0 View
I'm involved in a study of odor control technologies for municipal wastewater treatment plant. One of the control options involves a chemical 2-stage (acid/alkaline) packed bed scrubber. The...
03 March 2021 3,661 2 View
I am try to make the Paal Knorr reaction between 2.5 hexnedione and 6-amino hexanoic acid, my problem is type of solvent to use, because 6-hexaminohexanoic acid is soluble in water but I am not...
02 March 2021 4,443 2 View
I want to polymerize TEOS on a surface. I know that NH4OH is a preferred catalyst and an alcoholic solvent should be used .But I can not find certain amounts of each material to use. Does any one...
02 March 2021 1,404 6 View
Hi all, I need to cleave the ester in Ethyl 2-amino-1H-imidazole-5-carboxylate to make the carboxylic acid and retrieve the product from solution to use in downstream applications of linking to...
01 March 2021 8,766 3 View
Dear All, I want to quantify carbon deposition on the surface of the CuZnAl catalyst. I have tried thermogravimetric analysis, but I've got weight gain as the active Cu- get oxidised. Does anyone...
01 March 2021 1,907 3 View
I am doing a acid and a chiral amino alcohol reaction using DCC and HOBT in DCM or THF? Can anyone suggest me how to remove DCU and HOBT from a reaction mixture??
28 February 2021 2,153 1 View
hi everyone, I'm interested in the field of vaccine design specifically multi-epitope cancer vaccines , I want to know if there is a minimum and maximum number of epitopes we could use in a...
27 February 2021 3,882 3 View
I am working with Polyacrylic acid (100.000Da) and instead of water, I need to use another solvent (dioxane) to dissolve PAA. However, because of the high molecular weight, it's quite hard to...
25 February 2021 2,225 5 View
The limit test I'm referring to is USP method II. In this procedure you need to dropwise add 6N of NH4OH to the sample until it the pH is alkali. After that you need to dilute and add HOAc until...
23 February 2021 2,049 3 View
To do liquid biopsy and look for specific gene expressions there are so many published papers. Thera are different protocols and procedures used to isolate circulating cell free RNA or mRNA from...
23 February 2021 7,326 5 View