I have tried digestion of different concentration of TiO2 nanoparticles by using HF. The result I am getting is not uniform/ consistence. Also I want to know how to get the retained TiO2 from sand particles.
Use concentrated H2SO4 and heat the mixture (TiO2 + H2SO4) at temperature 400 C. TiO2 will dissolve stirring at 500 rpm.
Caution: Its a very dangerous and exothermic reaction. One should perform this experiment in fume hood ONLY!
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