I am using NiCo2S4/CNT compoiste with carbon nanotube paper as my current collecttor for the ASC device in KOH electrolyte. which behavior my CV curves shown and is its OK? attached is my CV curve plot
I need quick response from the scientists and research scholars and from doctors thanks a lot
Thank you for your comments and answers !!!!!!!
I think the important question you need to ask yourself is does your electrode material provide enhanced capacitive behaviour? In my opinion you are simply monitoring an oxidation process. There is very little capacitance in the potential range 0.0 V to 0.6 V (vs. ?).
Further to Ioannis Samaras 's question, which scan are you showing? Can you show the CVs for multiple scans? Do you have a reductive wave on the reverse sweep at any point (is it hidden under the trace)?
Your CV shows a very similar response to Figure 2 (glassy carbon electrode (GCE) WE, Ag/AgCl RE and Pt CE from the following article:
http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532015000901751
Jules
Also, try, if possible, somehow more skinny (thinner) WE(s), dear Muhammad Sajjad.
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