I am mainly working on magnetism but mostly having problems while their characterization using TEM and XRD could you please tell me that how can i interpret my results and what are the possible problems and newbies occurred while doing magnetic material characterization by TEM XRD and what are the other techniques of magnetic material characterization for defining their magnonic structure and domains................
Please specify the problem. With only this small amount of info I can't really think of any issues arising from XRD measurements that could be attributed to the magnetic properties of the material.
How did you take your TEM images? Some more clarity is required for suggestions
yes anil......he would have got beam deflection. He need to explain the specimen preparation and the material. SADP will be difficult, I feel.
What kind of problems did you already face? Can you please explain? Actually this very small information can't let people clearly know about the difficulty you faced.
One problem you can get in the TEM is your sample flying away, only to end stuck to the polepiece, it happened to us and it was a hell of a mess.. Anyway, generally speaking I think you'll find it more difficult to get good images, but for EDS analysis it should not be an issue..
With XRD you can index the patterns of the peaks and also you can identify them according to the structure. While getting images in TEM do focus on the magnification times. so that you can easily get actual size of the particles of your samples..
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