TEMPO "workup" without aqueous phase?

17 March 2023 1 7K Report

Do anyone know if it's possible to remove TEMPO, and how to do so, from an oxidation crude mixture through some sort of workup without using an aqueous phase? In this particular case, TEMPO elutes together with my compound, which is also highly soluble in aqueous phase.

Sunpish Weturai

i think use hydrazine in solid phase 2c and i not shure about that question i not good at its but tempo its look like gel

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