Please, can someone assist me with steps towards synthesising 2,9-dicarbaldehyde-1,10-phenanthroline from neocuproine using selenium dioxide?

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Andrzej Danel

Hi,

There are some procedures:

T.Letters 2013, vol 54, 4316-19

Heterocycles 2012, vol 86, 1419-29

Synth. Commun., 2003, vol 33, 475-480

Sincerely,

William Frost Berkowitz

Ditto:

Yong; Li, Bin; He, Hui; Wang, Shuao; Zhao, Yu-Liang; Chai, Zhi-Fang; Shi, Wei-Qun

Inorganic Chemistry (2014), 53(3), 1712-1720

Excellent Selectivity for Actinides with a Tetradentate 2,9-Diamide-1,10-Phenanthroline Ligand in Highly Acidic Solution: A Hard-Soft Donor Combined Strategy By Xiao, Cheng-Liang; Wang, Cong-Zhi; Yuan, Li-

Laventine, Dominic M.; Afsar, Ashfaq; Hudson, Michael J.; Harwood, Laurence M.

Heterocycles (2012), 86(2), 1419-1429.

Tuning the solubilities of bis-triazinylphenanthroline ligands (BTPhens) and their complexes

Bill

Emmanuel Ohaekenyem

thanks Danel and william