I have used the hydroxylamine method described in this paper:
Ōyanagui 1984 Reevaluation of assay methods and establishment of kit for superoxide dismutase activity: Analytical Biochemistry (142):290–296
But for a review of methods, including the hydroxyl amine method (and its shortcomings) see Beyer and Fridovich 1987 Assaying for superoxide dismutase activity: Some large consequences of minor changes in conditions. Analytical Biochemistry (161):559–566
Samrina: I can't find my copy of the paper, but I do have a procedure I wrote up that was based on the paper (and an earlier paper by Elstner and Heupel) that I will send to you. Good luck!