According to signalled reference, the samples can be etched electrolytically in HNO3 (conc.) + H2O (1:1 vol/vol; 9 V; 3 s): https://www.degruyter.com/view/j/afe.2012.12.issue-4/v10266-012-0118-6/v10266-012-0118-6.xml
You may find also useful the following paper: http://www.sciencedirect.com/science/article/pii/S1044580305002688