[About internal standard method using XRD for knowing the amount of zeolite in impurities.]
I want to know the amount of zeolite in impurities using internal standard method.
Alumina was selected as the standard sample、and made a calibration curve.
Usually,a calibration curve made from XRD is Straight line.
However my calibration curve is a beautiful curve(R^2=0.98)
What kind of problem can be considered?