What is the optimum temperature we need to maintain while pouring the H2So4 in PVA soln?
Subhasree Panda
The precipitate is formed as a result of salting out of PVA or the formation of an oxonium salt between PVA and sulfuric acid. Try
1.heat the mixture
2. reduce the concentration of sulfuric acid or PVA
3. add salting agents urea, thiourea, guadinium chloride
Thank you Yuri Mirgorod
Best wishes Subhasree Panda
Thank you @Yuri Mirgorod
Heating the mixture bit more than room temperature resulted in clear hydrogel
How to build a heterostructure in VESTA/VASP of two pristine materials having different space group and structure?
27 July 2024 739 2 View
What should be the zeta potential of bovine milk exosomes
25 July 2024 7,376 5 View
Any Upcoming call for papers in journals (SCI/SCIE indexed) related to image processing or computer vision. Special issues related to my area, whose submission dates are within a few months.
23 June 2024 5,021 1 View
Electron back scattered diffraction is a versatile tool for micro-structure and micro-texture analysis of a variety of materials e.g., metals/alloys, rocks, meteorites etc., EBSD completely works...
18 June 2024 1,477 5 View
I am working on a new polymer whose (hkl) values are not reported in the literature. How can I find out the (hkl) values of the XRD peaks?
17 June 2024 820 5 View
I have prepared some polymeric microspheres from chitosan and PCL. However while performing in vitro degradation study, I found difficulties in both above mentioned methods. Here I am mentioning...
20 May 2024 6,114 4 View
Hello guys, I am optimizing a perovskite photodetector device with the device structure ITO/PTAA/Cs0.15FA0.85PbI3/PCBM/BCP/Ag. PTAA (2 mg/mL): 5000 rpm/30 sec Perovskite (1.3 M): 1000 rpm/10...
10 May 2024 2,297 0 View
What is the mechanism behind increase in the peak intensity with filler loading in polymer nanocomposite. In my work, the (014) peak corresponding to the filler increased proportionately with...
08 May 2024 7,972 3 View
Hello guys, What might be the reason for getting two PL peaks after deposition of PCBM onto Cs0.15FA0.85PbI3 perovskite?
18 April 2024 5,169 0 View
Dear all, My device structure is ITO/PEDOT:PSS/Cs0.15FA0.85PbI3/PCBM/PEI/Ag. But till now, I am getting Jsc nearly 13. So please suggest to me how I can increase my Jsc and why I can not achieve...
13 March 2024 9,601 1 View
I got these smeared bands quite often lately. We typically run the gel at 140V with a 10-12% gel and do a wet transfer at 220 mA for 1.5 hr in cold room. We also noticed some dirty spots/dots (see...
10 August 2024 7,480 3 View
I have been working on Red blood cell-derived extracellular vesicles as Antisense Oligonucleotide (ASO) carriers. We normally run agarose gel to quantify the loading efficiency. I used naked ASO...
06 August 2024 3,130 2 View
I am having an issue with my gel image where my PCR product is not appearing very bright on the gel. When I perform gel extraction, the A260/280 purity value is very low. I used the Qiagen gel...
05 August 2024 9,798 3 View
SMEs are backbone of the country's white economy, most of them are II generation entrepreneurs and migrated from family owned business policies, and having sufficient higher educations for...
01 August 2024 5,562 2 View
Hello everyone, I performed a PCR yesterday, and the results showed no bands on the gel. Of course, I probably missed some crucial steps, like adding my samples to the PCR strips themselves, for...
31 July 2024 2,406 6 View
We are working on biopolymeric hydrogels. Our system is highly viscous and sticky, and the gel formed are high in strength. We are unable to use pH electrode and pH strip. Please suggest an easy...
30 July 2024 942 2 View
I am using CuBr/THPTA for a click reaction in total cell lysates. I am facing issues with my protein sample in non-reducing SDS-PAGE where it's not migrating properly and most of it remains at the...
29 July 2024 950 4 View
Since 2016 Brexit, the world needed to change the thinking behind traditional democracy as the democratic landscape changed, yet traditional democratic thinkers and actors have been acting as if...
28 July 2024 6,515 1 View
Liu Zhaosheng. 2003. Triassic and Jurassic sporopollen assemblage from the Kuqa Depression,Tarim Basin of Xinjiang,NW China. Palaeontologia Sinica, New Series A,no. 14(Whole no. 190)....
28 July 2024 6,390 1 View
I have tried to saturate ferritic steel with hydrogen using the electrolytic method and H2SO4. However, the effect was very poor even after 3 days of "saturation". Can anybody help in choosing a...
24 July 2024 4,393 2 View