So, add 0.0541g of Iron (III) chloride hexahydrate to 10ml ultrapure water.
You may weigh 0.0541g of Iron (III) chloride hexahydrate and transfer the Iron (III) chloride hexahydrate to a beaker of appropriate size. Add 5 mL of ultrapure water to the beaker to dissolve the salt. Transfer your solution to a 10 mL volumetric flask. Using ultrapure water, complete the solution's volume to reach 10 mL. You may prepare this solution on the day of the experiment.
It is better to prepare a fresh solution. This solution is sensitive to light.