How to perform Rietveld Analysis using XPert HighScore Plus Software?

More Rayappa Shrinivas Mahale's questions See All

female rats are not pregnant after observation of vaginal sperms ?

hello everyone , we are working on rat primary cortical neuronal cell culture for that we require a E18 pregnant rat , but after observing sperms the female rats were not pregnant what may be...

06 September 2018 2,015 3 View

Do human fibroblasts get transformed on S.C injection into mice?

I have injected human fibroblasts into mice. On harvesting the tumors, will I have a combination of mouse and human fibroblasts or human fibroblasts transformed into mouse like. How can they be...

23 November 2014 1,368 5 View

What is a good method for quantification of cell invasion in Organotypic cultures?

see above

20 February 2014 8,792 1 View

How to measure electrode potential?

I have prepared a nanometal composite film of 1micron thickness. I have to utilize it as an electrode for different purposes. For better understanding of it's electrochemical characteristics I...

03 February 2013 3,115 3 View

How to use metal powdered material as an electrode ?

In my current project I have to study various metal and metal composites to be used as electrodes in powder form. Can anyone suggest the suitable method to be applied? I am confused in...

05 December 2012 5,653 8 View

What could be the reason for XRD pattern starting from very high counts/intensity at 3 degree 2 theta?

I am working on XRD analysis of the clay minerals from the sea sediments. My XRD pattern shows very high counts at the start of the XRD pattern (3 degree 2 theta) which is very unusual. The counts...

31 January 2021 4,493 9 View

When i accept card in "HighScore plus app" should i attention to cards quality (in Reitveld analysis)?

Hi I wanna use Reitveld analysis in my project but i have big question that is: Should i see quality of each card (or Not important !!?), or it is enough to check the score and scale factor of...

04 January 2021 7,750 1 View

Which analysis method in XRD analysis is the most accurate way to measure crystallite size & lattice starin? Scherrer, Williamson-Hall or Rietveld?

Here are three different ways to calculate crystallite size and lattice strain of a sample, based on XRD peaks: "Scherrer" calculation, "Williamson-Hall" or "Rietveld". Each calculation is proper...

04 January 2021 7,836 4 View

Can I use Scherrer formula to calculate the crystallite size/Coherent domain size of Li2O5Si2 (lithium disilicate) from XRD data?

I`m comparing two different samples containing lithium disilicate and under SEM (5000x) there was a noted increase in the particle size (1st sample 2.7 microns in length and the 2nd sample 5...

28 October 2020 5,905 6 View

Why i am getting the ''no candidate found'' result whenever i search for the possible mineral peaks in Xpert Highscore software?

Currently i am working on Xpert Highscore XRD software for the estimation of clay minerals from the XRD pattern. However, whenever, i try to search minerals by using ''search and match''...

16 August 2020 3,069 4 View

Is the reported d-spacing value of particular mineral, a fixed value that can not vary in any software?

for example: if you consider the d-spacing of plagioclase's main peak in XRD which is at the d-spacing value 4.02, is it possible that this value may be reported as 4.021 or 4.0222, 4.017...

26 July 2020 709 3 View

Question about Rietveld refinement by highscore plus?

I am doing Rietveld refinement by highscore plus 3.0e, after refining scale factor, background, lattice parameters, W, U, V, peak shape and atomic coordinates, the GOF is good, but there are lots...

10 November 2019 1,620 5 View

is there any treatment necessary in xperthiscore to diffraction data from XRD to get FWHM in order to determine crystallite size, or simply import?

i want to measure the crystallite size and strains in powder sample processed through ball milling,but William-hall method could not be able to provide accurate size and strain.i am using Xpert...

03 April 2019 2,129 4 View

How to export rietveld refine data to ASCII format from highscore plus?

I have tried to convert the refined phase into ASCII format but I got only two columns rather than refined data, difference plot data. How can I get the complete refined data from high score plus...

02 March 2019 1,827 3 View

Unexpected peak spike up at around 64 degree (2theta)?

Dear respected RG members, Recently, we tried to prepare Ni doped MgO nanoparticles using co-precipitation method. The XRD pattern of pure MgO-NPs is going well with five peaks (20-80 degree). We...

20 January 2019 6,049 7 View

Gerhard Martens

Dear Rayappa Shrinivas Mahale ,

a detaild answer will cover a lot of text here.

Such work has been done already elsewhere.

The simplest thing for you is to have a look at approriate tutorials for example on youtube. Search by approriate buzz words...

Some search results:

https://www.youtube.com/watch?v=FpXUMUM-qn0

https://www.youtube.com/watch?v=GI3N3HVN3xc

https://www.youtube.com/watch?v=wDs6scvfof4

https://www.youtube.com/watch?v=lW5cwmqz_G4

You may also have a look at the answers of similar questions here on RG; for example:

https://www.researchgate.net/post/How_to_perform_rietveld_analysis_using_the_X_pert_high_score_plus_and_also_how_to_calculate_the_weight_percentage_of_austenite_and_martensite

Good luck and best regards

G.M.

Rayappa Shrinivas Mahale

@ Gerhard Martens Thank You Sir for your reply.

Michal Hegedus

Preferably, use some other software. I did not find Highscore useful at all. Go either for fullprof or JANA2020. There are free workshops for JANA2020 software and also very clear manual with examples is provided.

@ Michal Hegedus Thank You Sir for your suggestions.

Maykel Manawan

Michal Hegedus, how can you say that HSP isn't useful for Rietveld refinement? Do you have the software?

Abel Saka Gungure

Use Match software instead of high score

@ Abel Saka Gungure

Respected Sir Match software free version is available or we need to take licensed version?